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Idea Box for Smooth and Smart Experimentation vol. 1

We will introduce the trouble pre-detection conducted by additive manufacturers!

Useful systems have been established for conducting and analyzing experiments, such as utilizing experimental design methods and machine learning. On the other hand, one must think for themselves about what kind of experiments to set up. Here, we will introduce approaches that are useful in the experimental field for those who actually conduct experiments on coating, dispersion, application, and drying. This section will explain the prediction and prevention of risks before the use of additives. *For detailed content of the article, please refer to the PDF materials. For more information, feel free to contact us.*

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Idea Box for Smooth and Smart Experimentation Vol. 4

Successfully dispersing water-resistant treated flake pigments and pearlescent materials! Introducing flake pigments.

Paints and coatings using flake pigments and glitter materials, such as metallic and pearl colors, are enjoyable to look at. However, balancing performance aspects such as color development, design, particle orientation, sedimentation prevention, and water resistance can be quite labor-intensive. Typically, flake-shaped pigments overlap each other in the liquid. Especially in water-based systems, the surface is treated to be hydrophobic for water resistance, and if no action is taken, they do not disperse sufficiently in water. *For detailed content of the article, please refer to the PDF document. For more information, feel free to contact us.*

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Idea Box for Smooth and Smart Experimentation vol. 8

Using HazeGuard i makes it easy to evaluate dispersion in addition to the transparency of the film!

This is a tabletop measuring device developed to measure transparency. What makes it excellent is that, unlike conventional methods which only measured total light transmittance, it can measure separately for surface scattering and internal diffusion. Using a stable LED light source, it receives light that has passed through the sample film in an integrating sphere. Inside the integrating sphere, a combination of sensors and shutters allows for analysis that distinguishes between wide-angle scattering and narrow-angle scattering based on their arrangement. Additionally, if a dedicated cell is used, liquids can also be measured. *For detailed information, please refer to the PDF document. For more details, feel free to contact us.*

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Idea Box for Smooth and Smart Experimentation Vol. 2

Dispersion stabilization due to electrostatic repulsion is easily visible! Observing dispersed red pigment.

Regarding the stabilization of particle dispersion, it is explained that stabilization occurs due to electrostatic repulsion and steric hindrance. Stabilization through steric hindrance is a matter of nanoscale, so it is not visible. In contrast, electrostatic repulsion is relatively easy to understand, such as through zeta potential. However, there is also an impression that measurements from instruments yield numbers that are somewhat unclear. Here, we will introduce approaches that are useful in the experimental field for those who actually conduct coating, dispersion, application, and drying experiments. This section focuses on dispersion stabilization. *For detailed content of the article, please refer to the PDF materials. For more information, feel free to contact us.*

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Idea Box for Smooth and Smart Experimentation vol. 3

When choosing a dispersant, compatibility is the first step; now, let's introduce what the next key points are.

If the dispersant does not mix into the system, it will not distribute evenly in the liquid. First, compatibility is the primary point. Naturally, if it does not adsorb onto the surface of the particles that need to be dispersed, stabilization of the dispersion will not begin. The adsorption characteristics are the second point. In experiments, evaluations are conducted on the viscosity and particle size distribution of the dispersion, the viscosity and particle size distribution of the coating liquid, and the gloss, haze, transparency, and color name after application and drying. The third point is the evaluation in the final material system. *For detailed content of the article, please refer to the PDF document. For more information, feel free to contact us.*

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Idea Box for Smooth and Smart Experimentation vol. 5

Measurement of surface tension of membranes, do not misinterpret the data. Introducing approaches useful in the experimental field.

Very simple measuring devices are commercially available. This method measures surface tension and surface free energy from the contact angle of liquids. By dropping a liquid with known surface tension (such as water or cyclohexane) onto a coating or solid, the contact angle can be measured. The surface free energy (dispersive component, polar component, total) can be calculated from the contact angles of multiple liquids. *For more detailed information, please refer to the PDF document. Feel free to contact us for further inquiries.

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Idea Box for Smooth and Smart Experimentation Vol. 7

The key to highly reproducible viscosity measurements is to eliminate the history of the sample! There are various types of viscosity measurement devices.

In the laboratory, it is presumed that many viscosity measurements are conducted using B-type viscometers and rheometers capable of measuring viscoelastic behavior. It can be quite cumbersome, as the temperature must be controlled, and the equipment is delicate, requiring careful handling of the sample set. As a result, some researchers delegate the measurements to laboratory assistants and only receive the numerical data. However, it is important to note that simply matching the temperature is insufficient, and there may be questions about the reliability of the data. *For more detailed information, please refer to the PDF materials. Feel free to contact us for further inquiries.*

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